Validation data

Validation and robustness data for leaching tests

European Commission, Joint Research Centre, Held, A., García-Ruiz, S., Conneely, P., et al., Interlaboratory comparison to evaluate the precision of test methods for the assessment of the release of inorganic substances from construction products : horizontal dynamic surface leaching test CEN/TS 16637-2, horizontal up-flow percolation test CEN/TS 16637-3, analysis of inorganic substances in eluates CEN/TS 17195 and analysis of aqua regia digests CEN/TS 17201, Publications Office, 2020, https://data.europa.eu/doi/10.2760/288988

European Commission, Joint Research Centre, Conneely, P., Held, A., García-Ruiz, S., et al., Precision of test methods to assess the release of organic substances from construction products, Publications Office, 2020, https://data.europa.eu/doi/10.2760/772446

A.C. Garrabrants, D.S. Kosson, L. Stefanski, R. DeLapp, P.F.A.B. Seignette, H.A. van der Sloot, P. Kariher, and M. Baldwin. Interlaboratory Validation of the Leaching Environmental Assessment Framework (LEAF) Method 1313 and Method 1316. EPA 600/R-12/623 September 2012.   https://www.vanderbilt.edu/leaching/downloads/publications/leaf-supporting-documentation/

A.C. Garrabrants, D.S. Kosson, R. DeLapp, P. Kariher, P.F.A.B. Seignette, H.A. van der Sloot, L. Stefanski, and M. Baldwin. Interlaboratory Validation of the Leaching Environmental Assessment Framework (LEAF) Method 1314 and Method 1315. EPA 600/R-12/624 September 2012. https://www.vanderbilt.edu/leaching/downloads/publications/leaf-supporting-documentation/

Hjelmar, J. Hyks, A. Oberender, U. Kalbe, N. Bandow, A. van Zomeren and J. J. Dijkstra (2014). Additional Robustness Testing on TS-3 (CEN/TC 351/WG1). CEN/TC 351/WG 1 N 693. https://www.nen.nl/Standardization/Join-us/Technical-committees-and-new-subjects/TC-ConstructionBuilding/CENTC-351-EN.htm.

Hjelmar, J. Hyks, M. Wahlström, J. Laine-Ylijoki, A. van Zomeren, R. Comans, U. Kalbe, U. Schoknecht, O. Krüger, P. Grathwohl, T. Wendel, M. Abdelghafour, J. Méhu, N. Schiopu, M. Lupsea (2012) Robustness validation of TS-2 and TS-3 developed by CEN/TC351/WG1 to assess release from products to soil, surface water and groundwater. CEN/TC 351/WG 1/AHG N 214. https://www.nen.nl/Standardization/Join-us/Technical-committees-and-new-subjects/TC-ConstructionBuilding/CENTC-351-EN.htm

Kalbe, U., W. Berger and F.-G. Simon (2009). Results of German Ring Tests on the Validation of Leaching Standards for Source Term Determination. WASCON 2009: Sustainable Management of Wastes and Recycled Materials in Construction, Lyon, France, 3-5 June 2009.

Kalbe U., Berger W., Simon F.-G. (2008) Durchführung von Ringversuchen zur Validierung der Normen E DIN 19528 und E DIN 19529 (Ersatzbaustoffverordnung und Novellierung BBodSchV), Bundesanstalt für Materialforschung und -prüfung (BAM), Berlin, https://opus4.kobv.de/opus4-bam/frontdoor/index/index/docId/35475.

Kalbe U., Berger W., Eckardt J., Christoph G., Simon F.-G. (2007) Results of interlaboratory comparisons on the evaluation of the reproducibility of column percolation tests. J. Hazard. Mater. 148, 714-720.

Lopez Meza, S., Kalbe, U., Berger, W., & Simon, F. G. (2008). Harmonization and validation of leaching standards -new developments in Germany. Waste Management, 28(10), pp 1853-1867.[18] DIN 19528, Leaching of solid materials – Percolation method for the joint examination of the leaching behaviour of inorganic and organic substances.

López Meza S., Kalbe U., Berger W., Simon F.-G. (2008) Harmonization and validation of leaching standards – new developments in Germany. Land Contamination & Reclamation 16, 45-49.

H.A. van der Sloot, D.S. Kosson, A.C. Garrabrants, R. Comans and O. Hjelmar (2012) Parallel validation of CEN/TC292 characterisation leaching methods with USEPA validation. CEN/TC292/WG6/ N 1375.

H.A. van der Sloot, O. Hjelmar, J. Bjerre Hansen, P. Woitke, P. Lepom, R. Leschber, B. Bartet, N. Debrucker. Validation of CEN/TC 292 leaching tests and eluate analysis methods PrEN 12457 part 1 – 4, ENV 13370 and ENV 12506 in co-operation with CEN/TC 308. ECN-C–01-117.

H.A van der Sloot, G.J.L. van der Wegen, D. Hoede and G.J de Groot. Intercomparison of leaching tests for stabilized waste. In: Environmental aspects of Construction with waste materials. Eds. J.J.J.M. Goumans, H.A. van der Sloot, Th.G. Aalbers, Elsevier Science Publishers, Amsterdam, 1994. (Full report published as EUR Report 16133 EN (1994)), 63-76.

Yasutaka, A. Naka, H. Sakanakura, A. Kurosawa, et al., (2017). Reproducibility of up-flow column percolation tests for contaminated soils. PloS one, 12(6), e0178979.

 

More information on leaching references:

Background documents
Validation data
Leaching by material type
Grey literature
Useful weblinks

 

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